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A new approach is proposed to optimize some instrumental electrothermic parameters, i.e. injected volume, calcination duration, calcination and atomization temperatures, gas flow, in electrothermal atomic absorption spectrometry. It is based on the monitoring of the detection limit estimation variation by using an unconventional experimental design well adapted to a particular experimental domain...
A method, fast and simple to carry out, is proposed to optimize the instrumental spectroscopic parameters, such as bandpass, lamp current and monochromator slit height in electrothermal atomic absorption spectrometry. It is based on the monitoring of the detection limit estimation (DLE) variation by using a D-optimal experimental design. This method is tested on Cd, Mn, Cu and Sn. In comparison...
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