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Submicrometer‐sized poly(methyl methacrylate) (PMMA) particles were generated by precipitation with a compressed fluid antisolvent technique. The precipitation was carried out as follows. A solution containing PMMA was sprayed through a nozzle into a precipitator. The antisolvent CO2 was continuously passed through the precipitator during the operation at a flow rate of 2000 mL/min. When toluene was...
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