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Sugar‐based ionic surfactants forming micelles are known to suppress ESI of various compounds due to decrease in surface tension upon micelle formation []. For the first time, poly (sodium N‐undecylenyl‐α‐d‐glucopyranoside 4,6‐hydrogen phosphate, (poly‐α‐d‐SUGP) based surfactants with different chain lengths and head groups have been successfully synthesized, characterized, and applied as compatible...