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Evaporation of aqueous ammonia solutions of K7[Mo4Te4(CN)12]·12H2O or K6[W4Te4(CN)12]·5H2O, copper(ii) chloride, and ethylenediamine afforded the isostructural heterometallic complexes [{Cu(en)2}2{Cu(en)2(NH3)}{M4Te4(CN)12}]·5H2O (M = Mo or W), which were characterized by IR and ESR spectroscopy and X-ray diffraction analysis.
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