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We report structural studies of a chiral tridentate ligand which forms helical cubanes with cobalt(II) and manganese(II). A quadruple helicate with (P)‐chirality is obtained using a (S)‐ligand with cobalt(II) but the ligand binds manganese(II) in one of two possible orientations and either (P)‐ or (M)‐quadruple helicates may be observed for a given ligand enantiomer. The helicates may be linked into...