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Two new square planar Cu(II) and Ni(II) complexes, [CuL1(NCO)] (1) and [NiL2(N3)] (2) have been synthesized with two different tridentate N2O donor Schiff base ligands L1H (1:1 condensation product of benzoylacetone and 2-diethylaminoethylamine) and L2H (1:1 condensation product of benzoylacetone and 2-dimethylaminoethylamine), respectively. Both the complexes 1 and 2 have been characterized...