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An easy approach for the fabrication of titanium dioxide hollow spheres is proposed. Nanostructures were obtained by the conventional hard template method with silica-protected calcination. The samples were characterised by differential thermal analysis and thermogravimetry, Brunauer-Emmett-Teller nitrogen adsorption isotherms, X-ray diffraction, scanning and transmission electron microscopy (SEM...
In this work a very low cost and conventional technique was used to prepare Ge nano/microstructures by means of filling the material inside porous silicon (PS) using thermal evaporator. PS was prepared by anodization of Si wafer in ethanoic hydrofluoric acid (HF).The Ge layer was deposited onto the PS by thermal evaporation.Subsequent annealing at 650°C and 750 C for 30 mins were done to drive in...
Thin films of nanocrystalline CuGaS2 chalcopyrites have been prepared by chemical vapor transport (CVT) using elements of Cu, Ga, and S with iodine as the transporting agent. Crystalline layers of CuGaS2 have been grown using various iodine concentrations but with constant source materials, growth zones temperatures and growth durations. The films were grown onto sapphire (Al2O3) substrates. The deposits...
Size quantised cadmium sulphide (CdS) nanocrystalline thin films with different particle sizes and stoichiometric ratios were successfully grown on indium tin oxide substrates using an aqueous synthetic route. The effect of cadmium (Cd) to sulphur (S) ratio on the optical properties of CdS nanocrystalline films was investigated using EDAX, UV-vis spectroscopy, photoluminescence and Raman spectroscopy...
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