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Luminescent homoleptic dense 1,3‐benzodinitrile MOFs (metal–organic frameworks) of Eu3+ and Tb3+ were prepared from the anhydrous chlorides LnCl3 (Ln = Eu, Tb) and a melt of the linker ligand 1,3‐benzodinitrile [1,3‐Ph(CN)2=C6H4(CN)2]. The 1,3‐benzodinitrile ligands act as chemical scissors and cut down the LnCl3 structure to 2D sheets of trigonal Cl ion prisms around the rare earth ions and interlinks...
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