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An easily performed stepwise injection (SWIA) procedure based on on-line dilution of biodiesel samples and the formation of color-forming calcium (II) and magnesium (II) complexes with Eriochrome Black T (EBT) in an organic medium followed by spectrophotometric determination is presented. A sample of biodiesel was placed at the bottom of a mixing chamber connected to an automatic SWIA manifold. Isopropyl...
To determine the growth rate and element contents of fingernails in young adults, 109 apparently healthy college students were recruited for determination. As a result, the average growth rate of the left thumb was 3.14±0.63 mm/month with significantly faster rates in male and taller participants. The concentrations for Ca, Na, P, K, and Mg were 701.1±274.8 µg/g, 452.3±353.9 µg/g, 33l.6±119.7 µg/g,...
The unstability of EBT indicator solution results in the inaccuracy of the determination of calcium and magnesium. In this paper, surfactants are applied in EBT indicator solution, through spectrophotometric method, a stable EBT solution is obtained, and the precision of calcium and magnesium determination in water was improved. Moreover, surfactant PVA is used to determine calcium in the water of...
The study of blood serum for the content of Mg, K, Ca, Na, P and CI in blood serum was carried out on 47 healthy controls, 121 mentally handicapped, 27 psychiatric and 14 suffering from different somatic diseases. The patients were from Lublin, Zamość, Zwierzyniec, Krasnystaw, Łabunie, Ostrów Krupski. The study was carried out using atomie absorption spectrometer type Cobas Mira in the Central Laboratory...
Measurement of Na, K, Mg and Ca concentrations in natural fresh (non-mineralized) water samples can be performed in the same sample solution with little or no dilution, in acetylene-air flame with the addition of lanthanum chloride (La 15 g/L), caesium chloride (Cs 1.0 g/L) and hydrochloric acid (HCl 2.0% V/V) by flame atomic emission (Na, K) and absorption (Mg, Ca) spectrometry. Examined remaining...
Current Polish Standard methods for the determination of sodium, potassium, magnesium, and calcium in natural fresh water were compared with other official standards, mostly from the U.S. (ASTM, USEPA, USGS), regarding recommended top concentrations of measured elements in measured solutions and methods of regulating the sensitivity of measurements. Some of the disadvantageous limitations of conditions...
The phosphorus content of some animal protein sources was determined in order to identify the sample with the highest phosphorus content for use as a pilot sample. Varying concentrations of strontium and lanthanum were added to solutions of the ashed pilot sample for the determination of calcium and magnesium using flame atomic absorption spectrophotometry operated on the air-acetylene mode. At least...
The paper presents the results of determination of concentrations of chloride, sulfate, phosphate, ammonium, sodium, potassium, calcium and magnesium ions along with total nitrogen, pH and electrolytic conductivity for precipitation collected in nonindustrialized regions near Gdansk (Poland). A station used for the collection of samples of precipitation consisted of two substations, on of which was...
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