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Development of sustainable and economically viable methods is challenging but desired in organic synthesis. Herein, intramolecular C(sp3)–H imination between a free amine group and N‐methylene group is established using TBAI (20 mol %)‐TBHP (3.0 equiv.) in DMSO which is found to be an inexpensive replacement of PhI‐mCPBA in HFIP.
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