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A novel wet synthetic method utilizing weakly coordinating anions that yields LiCl‐free Zn‐based materials for hydrogen storage has recently been reported. Here we show that this method may also be applied for the synthesis of the pure yttrium derivatives, M[Y(BH4)4] (M=K, Rb, Cs). Moreover, it can be extended to the preparation of previously unknown thermodynamically unstable derivatives, Li[Y(BH...
A new wet chemistry method bypasses difficulties encountered in the preparation of complex metal borohyrides free from LiCl “dead mass” and it also solves all technical problems with a “one‐shot” metathetic reaction. The new reaction scheme utilizes metal cations and complex metal–borohydride anions, which are weakly solvated in organic solvents. It even allows for facile formation of thermodynamically...
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