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A novel method for the residue analysis of wine spoilage compound 2,4,6-trichloroanisole is reported. Wine (60ml) was extracted with 2ml toluene in presence of 24g MgSO 4 and 6g NaCl. Cleanup of the toluene phase by dispersive solid phase extraction with mixture of 100mg CaCl 2 , 25mg primary secondary amine and 50mg MgSO 4 was effective in minimising co-extractives and matrix...
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