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The reversible hydrogen storage properties of Ti-catalyzed NaAlH 4 (and associated Na 3 AlH 6 ) were studied as a function of Ti-content using a dry preparation technique consisting of the ball-milling of NaAlH 4 +TiCl 3 mixtures (0-9 mol.% TiCl 3 ). This process is believed to result in the in situ solid-state introduction of metallic Ti via the reduction...
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