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Structural and spectroscopic properties of solid dianil of 2-hydroxy-5-methyl-isophthaldehyde have been investigated. This is a Schiff base containing intramolecular O-H...N hydrogen bonding. Single crystal X-ray diffraction shows that the possibly equivalent hard structural parameters (bond lengths and the valence angles) of the title molecule are hardly differentiated by an asymmetric hydrogen bonding...
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