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A 2D network complex [Ag 2 (pydco)] n (1) (pydco=pyridine-2,6-dicarboxylic acid N-oxide) was synthesized and structurally characterized. Fluorescence spectrum of complex 1 and the free ligand indicates that the cooperative association of Ag–Ag contacts and the intraligand (π–π ∗ ) interactions lead to the unusual intense fluorescent emission upon photoexcitation.
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