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Low‐valent Ti‐mediated homolytic C−O bond cleavage offers unified access to carbon radicals from ubiquitous non‐activated tertiary, secondary, and even primary alcohols. In contrast to the representative Ti reagents, which were ineffective for this purpose, “TiCl2(cat)”/Zn (cat=catecholate) was found to be specifically active. This method was applied to the addition reactions of radicals to alkenes...
Low‐valent Ti‐mediated homolytic C−O bond cleavage offers unified access to carbon radicals from ubiquitous non‐activated tertiary, secondary, and even primary alcohols. In contrast to the representative Ti reagents, which were ineffective for this purpose, “TiCl2(cat)”/Zn (cat=catecholate) was found to be specifically active. This method was applied to the addition reactions of radicals to alkenes...
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