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Foldectures are typically formed from foldamers carrying a Boc group at the N‐terminus, which creates a network of N−H⋅⋅⋅O hydrogen bonds linking adjacent foldamers in head‐to‐tail packing modes. Although much less sterically demanding, cyclopropanoyl amides feature additionally an α‐proton known to form Cα−H⋅⋅⋅O hydrogen bonds with electron‐rich partners. Experimental and computational investigations...
The rational design of self‐assembling organic materials is extremely challenging due to the difficulty in precisely predicting solid‐state architectures from first principles, especially if synthons are conformationally flexible. A tractable model system to study self‐assembly was constructed by appending cyclopropanoyl caps to the N termini of helical α/β‐peptide foldamers, designed to form both...
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