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The first general examples of palladium‐catalyzed direct C−H olefination of polyfluoroarenes using alkenyl tosylates as electrophilic coupling partners are presented. By employing the Pd/L1 catalyst system (L1=N‐methyl‐2‐(2’,4’‐dimethoxyphenyl)‐3‐dicyclohexylphosphinoindole), the olefinated polyfluoroarenes can be obtained in good‐to‐excellent yields. Good structural and functional compatibility are...
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