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Nickel‐catalyzed reductive cross‐coupling of allylic difluorides with aryl iodides was achieved via allylic C−F bond activation. Based on this protocol, a series of γ‐arylated monofluoroalkenes were synthesized in moderate to high yields with high Z‐selectivities. Mechanistic studies suggest that the C−I bonds of the aryl iodides and the C−F bonds of the allylic difluorides were cleaved via oxidative...
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