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Zero‐dimensional (0D) nanospheres, 1D nanocaterpillars, and 3D aggregates are produced from simple diblock copolymers containing polyacetylene (PA) via in situ nanoparticlization of conjugated polymers. The diblock copolymers are prepared by ring‐opening metathesis polymerization via one‐pot sequential addition of an endo‐tricyclo[4.2.2.0]deca‐3,9‐diene (TD) and cyclooctatetraene. Initially, they...
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