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The solubility and self‐assembly behavior of poly(3‐hexylthiophene) (P3HT) in solvent mixtures, and the dominant intermolecular forces related to these attributes, have only been partially scrutinized. In this work, the extent of aggregation of amorphous P3HT and the structural order of P3HT aggregates (Mn ≈ 20 kDa and Mn ≈ 75 kDa) are investigated in 54 solvent mixtures of chloroform with acetone,...
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