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A one‐pot approach for the preparation of diblock copolymers consisting of polystyrene and polymyrcene blocks is described via a temperature‐induced block copolymer (BCP) formation strategy. A monomer mixture of styrene and myrcene is employed. The unreactive nature of myrcene in a polar solvent (tetrahydrofuran) at −78 °C enables the sole formation of active polystyrene macroinitiators, while an...
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