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This work reports a simple, direct, and easy route to prepare thin films between graphene‐like materials and two hexacyanometallates, based on metal cation modification in graphene oxide (GO) thin films obtained by the liquid/liquid interfacial route. The reaction between GO and Cu2+ or Fe3+ ions in aqueous solution yields GO/Cu2+ or GO/Fe3+, and the nature of the interactions between the GO and the...
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