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The adsorption of Cl - on a Cu(111) electrode surface in acidic chloride solutions was studied in situ by cyclic voltammetry and scanning tunneling microscopy (STM) and ex situ by ultrahigh vacuum based spectroscopies. The voltammogram shows adsorption and desorption peaks superimposed by the hydrogen evolution current. By a combination of X-ray photoelectron spectroscopy, ultraviolet photoelectron...
The adsorption of Cl - ions on a Cu(111) electrode was studied by UHV-based spectroscopies and by cyclic voltammetry. After standard UHV preparation the sample was transferred to an electrochemical cell. The shape of the voltammograms can be explained by a superposition of Cl - adsorption/desorption and a hydrogen reduction current, if an enhancement of the hydrogen reduction by...
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