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Perfluoroterphenyl, an organic n‐semiconductor, has been derivatized by short ω‐mercaptoalkyl chains to permit the formation of self‐assembled monolayers on semiconductor and coinage metal substrates. Because the perfluoroaryl rings are prone to nucleophilic attack, strategies for the introduction of the side chains had to be developed that avoid the use of any nucleophiles. Keeping this in mind,...
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