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Boron–dipyrrins (BODIPYs) have found widespread application in bioimaging and materials science. These applications require the tuning of the chemical and photophysical properties of the fluorophore through the introduction of functional groups at the BODIPY core. In this context, an approach to difunctionalized BODIPYs was explored. Oxidative nucleophilic substitution of hydrogen (ONSH) in the 3‐(α‐)position...
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