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The reaction of cis-2-(p-methylbenzoyl)-1-cyclohexanecarboxylic acid (1) and 2-aminoethanethiol furnished three 9b-p-tolylperhydrothiazolo[2,3-a]isoindolone isomers (2-4). The steric structures of the saturated cis (3, 4) and trans (2) isoindolones were determined by 1 H and 13 C NMR spectroscopy, including DNOE, DEPT and HSC measurements. In the two cis isomers, the steric...
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