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During our efforts toward the synthesis of naturally occurring polyprenylated polycyclic acylphloroglucinol using a AuI‐catalyzed 6‐endo dig carbocyclization, we isolated stable vinyllic gold intermediates. Optimization lead to isolated yields of up to 98 %, using 2‐(di‐tert‐butylphosphino)biphenyl as the ligand. This transformation is derived from a silyl rearrangement that can be fully controlled...
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