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A new metallocapped cyclodextrin (CD) was synthesized by the regioselective debenzylation, induced by diisobutylaluminium hydride (DIBAL‐H), of perbenzylated cyclodextrins. This reaction allowed for the efficient preparation of an unprecedented CD–salen type copper(II) complex. The electrochemical behavior of both the bound and unbound CD–salen compounds was investigated by cyclic voltammetry. Notably,...
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