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Two copper(II) complexes were synthesized from tridentate ligands involving a (Nquinoline,Nazo,Ophenol) donor set. The copper(II) ion is tetracoordinate with a chloride ion occupying the fourth position of the coordination sphere. Both X‐ray diffraction and electron paramagnetic resonance (EPR) spectroscopy reveal that the copper(II) ion geometry is square planar in 1. In contrast, significant tetrahedral...
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