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An artificial peptide with three pendant bipyridine (bpy) ligands on a palindromic backbone was designed and used to make multimetallic assemblies. The tripeptide is synthesized by addition of ligand‐substituted aminoethylglycine monomers to both ends of a bpy‐substituted diacid. The tripeptide was treated with CuII acetate, tetrafluoroborate, and nitrate salts, and the chelation stoichiometry was...
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