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A mechanistic and kinetic study of the ring‐opening polymerization of ϵ‐caprolactone (CL) in the presence of a poly(ethylene glycol) (PEG)/calcium hydride (CaH2) co‐initiation system was conducted in the bulk over a range of polymerization temperatures (70 − 133 °C). The resultant polycaprolactone‐block‐poly(ethylene glycol)‐block‐polycaprolactone (PCL/PEG/PCL) triblock copolymers were characterized...
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