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A new pyrochlore-type structure (Bi 1.56 Co 0.44 )(Sb 1.48 Co 0.52 )O 7 compound has been synthesized using ceramic method in air. Rietveld refinements using X-ray powder diffraction data confirmed an overall A 2 B 2 O 7 cubic pyrochlore structure with a=10.44896 (2)Å and Fd-3m symmetry. The reliability factors are R wp =3.09%;...
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