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The formation of Pd–Ag nanoparticles deposited from the heterobimetallic acetate complex PdAg2(OAc)4(HOAc)4 on α-Al2O3, γ-Al2O3, and MgAl2O4 has been investigated by high-resolution trans-mission electron microscopy, temperature-programmed reduction, and IR spectroscopy of adsorbed CO. The reduction of PdAg2(OAc)4(HOAc)4 supported on γ-Al2O3 and MgAl2O4 takes place in two steps (at 15–245 and 290–550°C)...
The formation of Pd–In catalysts synthesized from the heteronuclear acetate complex PdIn(CH3COO)5 was studied by temperature-programmed reduction, electron microscopy, IR spectroscopy of adsorbed CO and hydrogen temperature-programmed desorption (H2-TPD). IR spectroscopy of adsorbed CO and H2-TPD confirmed the formation of bimetallic Pd–In nanoparticles. It was found that the Pd–In nanoparticle surface...
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