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The redox activity of molecular phenazine catalysts has been previously exploited for aerobic oxidative amine homo‐ and cross‐coupling reactions. In this contribution, we have extended the reaction scope of this novel type of organocatalyst and used them in the cross‐dehydrogenative aza‐Henry coupling of isoquinolines with nitromethane under aerobic conditions. Additionally, we have designed and prepared...
The aerobic Cu/ABNO catalyzed oxidative coupling of alcohols and amines is highlighted in the synthesis of amide bonds in diverse drug‐like molecules (ABNO=9‐azabicyclo[3.3.1]nonane N‐oxyl). The robust method leverages the privileged reactivity of alcohols bearing electronegative hetero‐ atoms (O, F, N, Cl) in the β‐position. The reaction tolerates over 20 unique functional groups and is demonstrated...
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