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We report the electroanalytical detection of n‐butylamine at a nickel/carbon nanotube (Ni/CNT) composite. Scanning Electron Microscopy (SEM) characterisation of the composite demonstrated that it consisted of bulk nickel particles ca. 2 μm in diameter entangled in CNT bundles. The spontaneous formation of Ni(OH)2 was optimised, and comparison with a 3 mm nickel electrode showed that ca. 4 μg of the...
We report here an effective method for the fabrication of a large number of carbon nanotube (CNT) triode-type micro-cathodes. Our technique combines composite electroplating and micromachining, avoiding the tedious direct growth and the screen-printing procedures conventionally used to fabricate such structures. The emitter structure is characterized by uniform diameters and heights, as well as by...
In this study, we first present the experimental results that regard the direct growth of CNTs on a conical-type tungsten (W) tip and their electron emission properties, in terms of the catalyst materials such as a nickel (Ni) and a cobalt (Co) as well as their composition ratios. Sharpening of W-tips was done by electrochemical etch and their diameters were controlled to range from 5 mum down to...
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