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Allylic alcohols were exploited as synthetic precursors of γ‐keto sulfones. The reaction involved the one‐pot generation of α,β‐enones in situ from the allylic alcohols by using a PdII–dioxygen catalytic system and subsequent sulfa‐Michael addition in the presence of water. Importantly, water was identified as a sustainable substitute for a toxic copper salt to promote organosulfonyl addition. Diverse...
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