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For the first time, the β‐anomer of N‐acetylglucosamine derivative methyl 2‐acetamido‐3,4,6‐tri‐O‐benzyl‐2‐deoxy‐β‐D‐glucopyranoside (9b) was synthesized, isolated, and used in the synthesis of sugar‐based primary amine 4b. Sugar‐based primary amine 5a, an anomeric pair of monosaccharide derivatives 6a and 6b, and precursors to all these compounds were also synthesized, isolated, and well studied...
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