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Three diiron hexacarbonyl complexes (2, 3 and 4) with naphthalene-1,8-bis(thiolate) skeleton as their bridging linkages are reported. For comparison, the protonated form of complex 4 was also prepared (4H+). They bear respectively a functional group on the naphthalene ring at the position 2, i.e. −CH2OH (2), −COOH (3), −CH2N(Et)2 (4) and −CH2NH+(Et)2 (4H+). Complex 2 was derived from the direct reduction...
Electrochemical investigations and chemical reduction of the diiron hexacarbonyl complex bearing a 1,8-naphthalene moiety bridging linkage into which a ferrocenyl group was deliberately incorporated were performed. The complex exhibited two reduction and two oxidation processes in dichloromethane. Our results revealed that the first reduction could be assigned to an ECE (Electrochemical, Chemical...
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