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The power and precision of IR spectrometry, or IR quantitative spectroscopy, to observe water molecules embedded in macromolecules, is illustrated, taking as examples the determination of the structures of the hydrogen-bond network of a dried polysaccharide, hyaluronan, of a dried protein, bovine serum albumine, and of a dried polymer, a sulfonated polyimide. We also indicate how IR spectrometry conveys...
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