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A one-step synthesis of cyclohexanone acetals from phenol/alcohol mixtures has been explored using bifunctional aluminum borates supported Pd catalysts. Three aluminum borates have been prepared via either a high temperature calcination (9Al2O3·2B2O3) or a self-pressured thermal synthesis (PKU-1 and ABO-X) using various aluminum precursors and boric acid. Well dispersed Pd nanoparticles loaded on...
The effect of different catalysts (NaY, Cr-VPI-5, acidic kaolinite clay, clayfen, and p-toluenesulfonic acid) on the reaction between cyclohexanone and methanol-d 4 was investigated using GC-MS and in situ NMR spectroscopy at room temperature. An in situ IR spectroscopy analysis of pyridine adsorbed on the clay and NaY samples showed that they are both weakly acidic. Depending on the catalyst...
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