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Vapour deposition of Pd with CO background pressure onto an ordered alumina film kept at 90 K results in the formation of a palladium carbonyl-like compound. The growth and decomposition of this Pd x (CO) y species is investigated using SPA-LEED (spot-profile analysis), thermal desorption spectroscopy (TDS) and photoemission of both core and valence levels. It is found that the nucleation...
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