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The reaction of Pd II (μ-OOCMe) 4 M II (OH 2 ) (M=Ni, Co, Mn) with azobenzene under mild conditions produces the homonuclear complex with ortho-metallated azobenzene (PhN=NC 6 H 4 ) 2 Pd 2 (μ-OOCMe) 2 (4) in higher than 90% yield as the sole Pd-containing reaction product, while the co-metals are recovered as the corresponding...
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