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The mechanochemical cycloreversion of 1,2,3‐triazole compounds, which serve as unusually stable building blocks in materials and biomolecular chemistry as a result of mild “click chemistry”, remains puzzling. We show that the hitherto discussed straight‐forward retro‐click mechanism of the 1,4‐disubstituted isomer, even if CuI catalyzed, can be ruled out in view of more favorable activation free energies...
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