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A new method was optimized for the determination of emerging Fusarium mycotoxins enniatins (ENs) and beauvericin (BEA) in different types of water. Mycotoxin analysis was performed by dispersive liquid-liquid microextraction (DLLME) combined with liquid chromatography-tandem mass spectrometry (LC-MS/MS). Mycotoxins were efficiently extracted from water into carbon tetrachloride by DLLME technique...
An analytical method was developed using ultra-high-pressure liquid chromatography–triple quadrupole-tandem mass spectrometry (UHPLC–TQ-MS/MS) to simultaneously analyze 14 sulfonamides (SA) in 6min. Despite the rapidity of the assay the system was properly re-equilibrated in this time. No carryover was observed even after high analyte concentrations. The instrumental detection limit based on signal-to-noise...
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