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l‐Alanyl‐glutamine dipeptide assembles with CuII ions to give the 2D coordination framework [Cu2(C8H13N3O4)2·2H2O]n (1) in which amino acid residues result in specific void space. In presence of 4,4′‐bipyridine, framework 1 is turned into a binuclear complex [Cu2(C8H13N3O4)2(H2O)2(C10H8N2)·8H2O] (2), which is further linked into a 2D hydrogen‐bonded layer in which amino acid residues induce a hydrogen‐bonded...
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