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Functional coordination polymers are commonly prepared by solution reactions. In the current study, however, a method to prepare amorphous coordination polymers by photoirradiation of liquids was developed. UV irradiation of transparent ionic liquids containing cationic ruthenium sandwich complexes produced yellow microporous coordination polymers exhibiting gas adsorption properties. More information...
Ruthenium‐containing organometallic ionic liquids with the B(CN)4 anion were developed that generate microporous amorphous coordination polymers upon UV irradiation. UV light irradiation of [Ru(C5H5)(C6H5R)][B(CN)4] (R=butyl, ethyl, octyl) quantitatively generated a yellow powder of a coordination polymer with the formula [Ru(C5H5){B(CN)4}]n. In this reaction, the arene ligand is eliminated by UV...
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