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Sulfur dioxide (SO2)‐based gas therapy and chemodynamic therapyare both reactive oxygen species (ROS)‐mediated anticancer strategies, but there are few reports of their combined application. To this end, a novel graft‐type copolymeric SO2 prodrug, PLG‐g‐mPEG‐DNs, is designed and synthesized in this work. The amphiphilic polypeptides can self‐assemble into nanoparticles (NPs) and encapsulated Cu(II)...