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We report on the synthesis and characterization of a family of three water‐soluble bola‐amphiphilic zinc‐porphyrin‐perylenebisimide triads containing oligo carboxylic‐acid capped Newkome dendrons in the periphery. Variations of the perylenebisimide (PBI) core geometry and dendron size (G1 and G2 dendrons with 3‐ and 9‐carboxylic acid groups respectively) allow for tuning the supramolecular aggregation...