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A novel series of spirofused indoloquinuclidines was obtained by a tandem Pictet–Spengler/AuI‐catalyzed cyclization sequence. By combining N‐propargyl tryptamine with aldehydes in the presence of acetic acid and a gold complex, the target indoloquinuclidines were obtained. The combination of a chiral phosphoric acid catalyst for the asymmetric Pictet–Spengler reaction with a gold complex furnished...
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